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(R)-3-(5-chloroindole-2-carbonylamino)-3,4-dihydrocarbostyril → (s)-3-(5-Chloroindole-2-carbonylamino)-1-methyl-3,4-dihydrocarbostyril
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (R)-3-(5-chloroindole-2-carbonylamino)-3,4-dihydrocarbostyril | HCID 9840862 | — |
| 反応物 | (R)-3-(5-chloroindole-2-carbonylamino)-1-methyl-3,4-dihydrocarbostyril | HCID 44357938 | — |
| 反応物 | (R)-3-t-butyloxycarbonylamino-3,4-dihydrocarbostyril | HCID 69198597 | — |
| 生成物 | (s)-3-(5-Chloroindole-2-carbonylamino)-1-methyl-3,4-dihydrocarbostyril | HCID 44357937 | — |
反応手順
The title compound was prepared from (S)-3-t-butyloxycarbonylamino-3,4-dihydrocarbostyril (prepared in Example 5) by the procedures described for the preparation of (R)-3-(5-chloroindole-2-carbonylamino)-1-methyl-3,4-dihydrocarbostyril (Example 14) from (R)-3-t-butyloxycarbonylamino-3,4-dihydrocarbostyril. HPLC/MS [M+H]+, 354.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07425550B2 |
| 出典データセット | uspto-grants-2008_09 |
| ORD ID | ord-43c4639d8ae24264a154cd6b8126972c |
| 出典メモ | uspto-grants-2008_09 |