化工社化工社 化学情報印刷レポート · 研究参考用
Methyl L-threoninate hydrochloride → HCID 22895021、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl L-threoninate hydrochloride | HCID 2734893 | — |
| 反応物 | N-(3-Nitrophenylacetyl)-L-alanine | HCID 53788870 | — |
| 溶媒 | Chloroform methanol | HCID 21584188 | — |
| 生成物 | HCID 22895021 | HCID 22895021 | — |
反応手順
Following General Procedure C and using N-(3-nitrophenylacetyl)-L-alanine (from Example D11 above) and L-threonine methyl ester hydrochloride (Aldrich), the title compound was prepared as a solid. The reaction was monitored by tlc (Rf=0.1 in 95:5 CHCl3/MeOH) and the product was purified by silica gel chromatography using 95:5 CHCl3/MeOH as the eluent.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06211235B1 |
| 出典データセット | uspto-grants-2001_04 |
| ORD ID | ord-d9d0beb436cd4a5f971e6fbfd0a1a608 |
| 出典メモ | uspto-grants-2001_04 |