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Chloroform → 3-[3-(4-Pentadecenylamino)benzoyl]-4-carboethoxythiazolidine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Chloroform | HCID 6212 | — |
| 反応物 | Triethylamine | HCID 8471 | — |
| 反応物 | Ethyl thiazolidine-4-carboxylate | HCID 103574 | — |
| 反応物 | 3-(4-Pentadecenylamino)benzoyl chloride hydrochloride | HCID 73708083 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | 3-[3-(4-Pentadecenylamino)benzoyl]-4-carboethoxythiazolidine | HCID 53862308 | — |
反応手順
One-tenth mole of 3-(4-pentadecenylamino)benzoyl chloride hydrochloride in methylene chloride is added to a solution of 0.1 mole of ethyl thiazolidine-4-carboxylate in chloroform containing two equivalents of triethylamine. After 5 hours at 20° C. the solution is filtered and evaporated to a white solid which is recrystallized from acetonitrile.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04440940 |
| 出典データセット | uspto-grants-1984_04 |
| ORD ID | ord-d8d93525a0534249b649b99e88de8c61 |
| 出典メモ | uspto-grants-1984_04 |