化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → Enoxacin hydrochloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Enoxacin | HCID 3229 | — |
| 生成物 | Enoxacin hydrochloride | HCID 12901163 | — |
反応手順
The anhydrous AT-2266 prepared by Reference Example 2 or the AT-2266.trihydrate prepared by Reference Example 3 was dissolved in 5% hydrochloric acid and the solution was concentrated to dryness under reduced pressure. The residue was recrystallized from water to give the AT-2266.hydrochloride, mp above 300° C. (dec.).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04442101 |
| 出典データセット | uspto-grants-1984_04 |
| ORD ID | ord-118b83e619ae4bc79b78fd600e7791e7 |
| 出典メモ | uspto-grants-1984_04 |