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Ethyl 2-(4-hydroxyphenoxy)-2-methylpropanoate → Ethyl 2-methyl-2-[4-(6-chloroquinolin-2-yloxy)phenoxy]-propionate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl 2-(4-hydroxyphenoxy)-2-methylpropanoate | HCID 181741 | — |
| 反応物 | 2,6-Dichloroquinoline | HCID 607502 | — |
| 生成物 | Ethyl 2-methyl-2-[4-(6-chloroquinolin-2-yloxy)phenoxy]-propionate | HCID 20461951 | — |
反応手順
Ethyl 2-methyl-2-[4-(6-chloroquinolin-2-yloxy)phenoxy]-propionate (36) was prepared from 2,6-dichloroquinoline and ethyl 2-methyl-2-(4-hydroxyphenoxy)propionate following essentially the same procedure as that described in Example 1. The product was isolated after chromatography as a low melting point solid. Mass spectrum (m/e): 385 (parent ion; 30%); 312 (35%); 271 (100%); 270 (100).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04444584 |
| 出典データセット | uspto-grants-1984_04 |
| ORD ID | ord-1a94effe0ac8457cbaabccc480144319 |
| 出典メモ | uspto-grants-1984_04 |