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4-Chloro-2-phenyl-pyrimidine-5-carboxylic acid benzylamide → HCID 178418303、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Chloro-2-phenyl-pyrimidine-5-carboxylic acid benzylamide | HCID 53937500 | — |
| 反応物 | Sodium hydrogen sulphide | HCID 86586439 | — |
| 生成物 | HCID 178418303 | HCID 178418303 | 65.2% |
反応手順
Using the procedure from Preparation 34, 5.8 g (17.9 mmol) of 4-chloro-2-phenyl-pyrimidine-5-carboxylic acid benzylamide was reacted with 5.1 g (72 mmol) of sodium hydrogen sulfide to give 3.75 g of the title compound, mp 189°-193° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05733921 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-73bd32edf0dc4454ae0af2e0d20af183 |
| 出典メモ | uspto-grants-1998_03 |