化工社化工社 化学情報印刷レポート · 研究参考用
1-Bromo-4-(methylsulphonyl)benzene → 4-(4-Methanesulfonyl-phenyl)piperazine-1-carboxylic acid tert-butyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Bromo-4-(methylsulphonyl)benzene | HCID 77014 | — |
| 反応物 | tert-Butyl piperazine-1-carboxylate | HCID 143452 | — |
| 生成物 | 4-(4-Methanesulfonyl-phenyl)piperazine-1-carboxylic acid tert-butyl ester | HCID 59793501 | — |
反応手順
The title compound was prepared according to the procedure described for example AX from 4-bromophenyl methyl sulfone and N-Boc-piperazine (31%, white solid, MS (m/e): 241.2(M-Boc, 100%)
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07427612B2 |
| 出典データセット | uspto-grants-2008_09 |
| ORD ID | ord-cbe02993323f47e199ad3f2ba96f5502 |
| 出典メモ | uspto-grants-2008_09 |