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Benzene → 2,3-Dichlorophenyl sulfamate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzene | HCID 241 | — |
| 反応物 | 2,3-Dichlorophenol | HCID 11334 | — |
| 反応物 | Chlorosulfonyl isocyanate | HCID 70918 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | 2,3-Dichlorophenyl sulfamate | HCID 54352588 | 72% |
反応手順
This compound was prepared according to the procedure of Example 84. Thus, a mixture of 16.3 g (0.10 mole) of 2,3-dichlorophenol and 9.1 ml (0.105 mole) of chlorosulfonyl isocyanate in 75 ml of toluene gave 17.4 g (72%) of the title compound as an off-white solid, mp 116°-117° C. (benzene).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05273993 |
| 出典データセット | uspto-grants-1993_12 |
| ORD ID | ord-90931d6a25ac4c54a78f345978ebacff |
| 出典メモ | uspto-grants-1993_12 |