化工社化工社 化学情報印刷レポート · 研究参考用
Phenol → Phenyl 3-(o-tolyl)propanoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phenol | HCID 996 | — |
| 反応物 | 3-(2-Methylphenyl)propanoyl chloride | HCID 13029201 | — |
| 生成物 | Phenyl 3-(o-tolyl)propanoate | HCID 86715420 | 93% |
反応手順
The procedure as described in Example 4a) was repeated with phenol (48 mmol) and 3-o-tolylpropanoyl chloride (55 mmol). The crude product (12.4 g, 97%) was short path distilled at 127-129° C./0.05 mbar to yield 10.6 g (93%) of product as a colourless, semicrystalline oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08877704B2 |
| 出典データセット | uspto-grants-2014_11 |
| ORD ID | ord-653a29921ad541cd957e9893431a59c5 |
| 出典メモ | uspto-grants-2014_11 |