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5-Nitrofuroyl chloride → 5-nitro-N-[2-(piperidin-1-yl)phenyl]furan-2-carboxamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-Nitrofuroyl chloride | HCID 90711 | — |
| 反応物 | 2-(Piperidin-1-yl)aniline | HCID 458795 | — |
| 生成物 | 5-nitro-N-[2-(piperidin-1-yl)phenyl]furan-2-carboxamide | HCID 2995620 | 100% |
反応手順
The compound was prepared according to the procedure described in Example 2 from 5-nitro-furan-2-carbonyl chloride and 2-piperidinoaniline. Yield: 100%. MS: 316 (M+1). LC/MS purity: 100%. 1HNMR (CDCl3, 300 MHz): δ 8.2 (d, 1H), 7.85 (d, 1H), 7.55 (m, 1H), 7.4 (m, 3H), 3.8-3.2 (bm, 4H), 2.7-1.9 (bm, 6H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07429603B2 |
| 出典データセット | uspto-grants-2008_09 |
| ORD ID | ord-a048a0ae055d459d856eeafc414d3f81 |
| 出典メモ | uspto-grants-2008_09 |