化工社化工社 化学情報印刷レポート · 研究参考用
Methylhydrazine → 1-Boc-1-methylhydrazine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methylhydrazine | HCID 6061 | — |
| 反応物 | Di-tert-butyl dicarbonate | HCID 90495 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 1-Boc-1-methylhydrazine | HCID 3748280 | — |
反応手順
10 mL of methyl hydrazine was dissolved in 90 mL of ethanol, and under stirring at ice-cooling, a solution of 41 g of di-tert-butyldicarbonate in 90 mL of ethanol was added dropwise over 45 minutes. After stirring at room temperature for 7 hours, the solvent was evaporated, to afford 24.7 g of the title compound as a colorless oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07429609B2 |
| 出典データセット | uspto-grants-2008_09 |
| ORD ID | ord-fc6875eeb4de43a8bab93f777795ac96 |
| 出典メモ | uspto-grants-2008_09 |