関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 3-Methyl-1-butene | HCID 11239 | — |
| 反応物 | Hexafluoroacetone | HCID 12695 | — |
| 生成物 | 5-Hydroxy-2-methyl-6,6,6-trifluoro-5-trifluoromethylhex-2-ene | HCID 12783437 | — |
反応手順
A stirred mixture of hexafluoroacetone (235 g) and 3-methylbut-1-ene (100 g) was heated at 125° C. under a pressure of 17 atmospheres for a period of 20 hours. Distillation of the product mixture under reduced pressure yielded 5-hydroxy-2-methyl-6,6,6-trifluoro-5-trifluoromethylhex-2-ene as a mobile colourless liquid, b.p. 43° C./15 mm Hg.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04378316 |
|---|
| 出典データセット | uspto-grants-1983_03 |
|---|
| ORD ID | ord-65cee0cebf8e4d50ac625714b60261fb |
|---|
| 出典メモ | uspto-grants-1983_03 |
|---|
