化工社化工社 化学情報印刷レポート · 研究参考用
Triethylamine → Benzoic acid, 4-(phenylmethoxy)-, 1-(trifluoromethyl)nonyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Triethylamine | HCID 8471 | — |
| 反応物 | 2-Dimethylaminopyridine | HCID 21885 | — |
| 反応物 | 4-Benzyloxybenzoylchloride | HCID 3766410 | — |
| 反応物 | 1,1,1-Trifluorodecan-2-ol | HCID 3864464 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | Benzoic acid, 4-(phenylmethoxy)-, 1-(trifluoromethyl)nonyl ester | HCID 14745753 | — |
反応手順
In 10 ml of methylene chloride was dissolved 1.23 g of 4-benzyloxybenzoic acid chloride, and a solution of 0.96 g of optically active 1,1,1-trifluoro-2-decanol, 0.55 g of dimethylaminopyridine, and 0.48 g of triethylamine in 20 ml of methylene chloride was added thereto in small portions under ice-cooling.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05837163 |
| 出典データセット | uspto-grants-1998_11 |
| ORD ID | ord-e3855fb1692746578a81a23d6531ab26 |
| 出典メモ | uspto-grants-1998_11 |