化工社化工社 化学情報印刷レポート · 研究参考用
Hydroxylamine → Benzohydroxamic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydroxylamine | HCID 787 | — |
| 反応物 | Benzoyl chloride | HCID 7412 | — |
| 反応物 | Sodium Bicarbonate | HCID 516892 | — |
| 溶媒 | Ethyl Acetate | HCID 8857 | — |
| 生成物 | Benzohydroxamic acid | HCID 10313 | — |
反応手順
To 281 mg of the compound (6) were added 2 ml of ethyl acetate, 2 ml of aqueous saturated sodium hydrogencarbonate, and 0.077 ml of benzoyl chloride and the mixture was reacted at room temperature for 1. 5 hours to obtain a benzoylamino-alcohol compound (compound (7), C51H63NO13Si, molecular weight of 926.14).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06136990 |
| 出典データセット | uspto-grants-2000_10 |
| ORD ID | ord-7adc17dd78964447b9f8aeb642f7f612 |
| 出典メモ | uspto-grants-2000_10 |