化工社化工社 化学情報印刷レポート · 研究参考用
Water → HCID 178419936、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | 2-Naphthalenecarbonitrile | HCID 11944 | — |
| 反応物 | Sodium Azide | HCID 33557 | — |
| 反応物 | Lithium Chloride | HCID 433294 | — |
| 溶媒 | 2-Methoxyethanol | HCID 8019 | — |
| 生成物 | HCID 178419936 | HCID 178419936 | — |
反応手順
A mixture of 10 g of 2-cyanonaphthalene, 10.61 g of sodium azide, and 7.67 g of lithium chloride was placed in a reaction vessel, and 240 ml of 2-methoxyethanol serving as a solvent was added thereto. The above mixture was refluxed with stirring for 80 hours. The mixture was cooled to room temperature, and 500 ml of water was added to the mixture.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05420288 |
| 出典データセット | uspto-grants-1995_05 |
| ORD ID | ord-28f1ea35b4c54d3e98646f4aae82b802 |
| 出典メモ | uspto-grants-1995_05 |