化工社化工社 化学情報印刷レポート · 研究参考用
Ethanol → Sodium 4-allyloxyphenylsulfonate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | Allyl bromide | HCID 7841 | — |
| 反応物 | Sodium benzenesulfonate | HCID 517327 | — |
| 溶媒 | Sodium Hydroxide | HCID 14798 | — |
| 生成物 | Sodium 4-allyloxyphenylsulfonate | HCID 86748076 | — |
反応手順
30 g of sodium phenylsulfonate are dissolved in 60 ml of ethanol and 50 ml of 15% sodium hydroxide, 20 g of allyl bromide are added and the mixture is refluxed for 48 hours. The ethanol is concentrated and the precipitate obtained is filtered off and then dried under vacuum in the presence of phosphorus pentoxide to give 23.3 g of the expected product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05481005 |
| 出典データセット | uspto-grants-1996_01 |
| ORD ID | ord-a77c4c4bb86f4f6896706e2d2950ecd9 |
| 出典メモ | uspto-grants-1996_01 |