関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 3-Methyl-2-butanone | HCID 11251 | — |
| 反応物 | 4-Methoxyphenylhydrazine hydrochloride | HCID 2723904 | — |
| 溶媒 | Acetic Acid | HCID 176 | — |
| 生成物 | 5-Methoxy-2,3,3-trimethyl-3H-indole | HCID 11095392 | — |
反応手順
To 4-methoxyphenyl hydrazine hydrochloride (4.84 g) was added 3-methyl-2-butanone (6.4 ml) and acetic acid (45 ml). The mixture was heated to 10° C. for 2.5 hours after which time the solvent was removed by rotary evaporation. Flash column chromatography gave the product (4.66 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US08378120B2 |
|---|
| 出典データセット | uspto-grants-2013_02 |
|---|
| ORD ID | ord-0f58494c1ef14cdc90d2e0dcd78b2684 |
|---|
| 出典メモ | uspto-grants-2013_02 |
|---|
