関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Methacrylic Acid | HCID 4093 | — |
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | Silane, (chloromethyl)trimethyl- | HCID 75361 | — |
| 溶媒 | Dimethylazanide | HCID 182180 | — |
| 生成物 | Methacryloxymethyltrimethylsilane | HCID 2760855 | — |
反応手順
300 mmol of Methylacrylic acid (MAA) and 200 mmol of chloromethyl trimethylsilane were dissolved in 400 ml of dimethylamide. Potassium carbonate was added to the solution and heated to 90° C. and stirred for 5 hours. Next, the reaction solution was filtered. The filtrate was added to a sodium hydrogen carbonate solution, extracted with ether and pure water respectively, dried, filtered, and concentrated to obtain trimethylsilanylmethyl methylacrylate (TMSA) having the formula (i) below
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06800420B2 |
|---|
| 出典データセット | uspto-grants-2004_10 |
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| ORD ID | ord-89374aab0d65459ebc755dc684689d3d |
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| 出典メモ | uspto-grants-2004_10 |
|---|
