化工社化工社 化学情報印刷レポート · 研究参考用
p-n-Octadecyloxybenzoic acid → 4-(trans-2-Decenyloxy)-benzoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | p-n-Octadecyloxybenzoic acid | HCID 139993 | — |
| 反応物 | Lithium hydroxide, monohydrate | HCID 168937 | — |
| 反応物 | Methyl-4-(trans-2-decenyloxy)-benzoate | HCID 18521070 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 4-(trans-2-Decenyloxy)-benzoic acid | HCID 18521013 | — |
反応手順
The ester 35g 565 mg, 1.95 mmol), and lithium hydroxide monohydrate (817 mg, 19.5 mmol) in 20 ml methanol were reacted according to the procedure for compound 36a. The yield was 482 mg (89% of a white powder.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06569504B1 |
| 出典データセット | uspto-grants-2003_05 |
| ORD ID | ord-ccede109ff2a4b66956b2756cfc70ce9 |
| 出典メモ | uspto-grants-2003_05 |