関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Triphenylphosphine | HCID 11776 | — |
| 反応物 | Pentafluorobenzyl bromide | HCID 74484 | — |
| 溶媒 | Diethyl Ether | HCID 3283 | — |
| 生成物 | (2,3,4,5,6-Pentafluorophenyl)methyl-triphenyl-phosphonium;bromide | HCID 21282127 | — |
反応手順
The toluene solution from Stage 1 was mixed with triphenyl phosphine (1 g) and heated at 130° C. for 3 hours. After cooling, the solution was diluted with diethyl ether (5 cm3) and the title compound filtered off, washed with hexane (4×5 cm3) and dried by suction.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04791139 |
|---|
| 出典データセット | uspto-grants-1988_12 |
|---|
| ORD ID | ord-071913ea308748ad9b60322c80e9fd44 |
|---|
| 出典メモ | uspto-grants-1988_12 |
|---|
