化工社化工社 化学情報印刷レポート · 研究参考用
2-Oxoglutaric Acid → 1,4,5,6-Tetrahydro-6-oxo-3-pyridazinecarboxylic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Oxoglutaric Acid | HCID 51 | — |
| 反応物 | Hydrazine | HCID 9321 | — |
| 生成物 | 1,4,5,6-Tetrahydro-6-oxo-3-pyridazinecarboxylic acid | HCID 99621 | 99% |
反応手順
The disclosed embodiments stem from the examination of several classes of compounds that quantitatively react with hydrazine to form stable organic products. The reaction of 2-ketoglutaric acid with hydrazine reacts to provide a greater than 99% yield of 6-oxo-1,4,5,6-tetrahydro-pyridazine-3-carboxylic acid (PCA) based on hydrazine as the limiting reagent. It has been found that this compound allows for the facile remediation of hydrazine under a variety of conditions. The focus of the disclosed embodiments concerns the use of 2-ketoglutaric acid or other dicarbonyl compounds for the remediation of hydrazine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08535430B2 |
| 出典データセット | uspto-grants-2013_09 |
| ORD ID | ord-e3234c6d563d46798823285107d150ba |
| 出典メモ | uspto-grants-2013_09 |