化工社化工社 化学情報印刷レポート · 研究参考用
1-Bromo-4-methoxybutane → Phenazine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Bromo-4-methoxybutane | HCID 521168 | — |
| 反応物 | 1-Phenazinol | HCID 135412648 | — |
| 生成物 | Phenazine | HCID 4757 | — |
| 生成物 | Ethoxyethane;phenazine | HCID 67351390 | — |
反応手順
Scheme 6 illustrates the synthesis of N-ethyl phenazine 1-hydroxybutyl methyl ether. The phenazine ether (21) is prepared by the alkylation of the 1-hydroxyphenazine (1) with 4-methoxybutylbromide (Aldrich Chemical Company, USA) to give phenazine derivative (21). N-ethyl phenazine (22) is prepared by reaction of compound (21) with diethyl sulfate in the presence of potassium carbonate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08535511B2 |
| 出典データセット | uspto-grants-2013_09 |
| ORD ID | ord-e25732e929014617bb8a9f0d336395cb |
| 出典メモ | uspto-grants-2013_09 |