化工社化工社 化学情報印刷レポート · 研究参考用
Sodium Hydroxide → Aluminum
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | Aluminum chloride, hexahydrate | HCID 24564 | — |
| 反応物 | HCID 10233207 | HCID 10233207 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Aluminum | HCID 5359268 | — |
| 生成物 | HCID 10233207 | HCID 10233207 | — |
反応手順
A portion of the above pure diisobutylphosphinic acid (135.01 g, 0.758 mol) was mixed with water and neutralized with dilute aqueous sodium hydroxide solution. The neutralized product was then mixed with a solution of 61.83 g (0.256 mol) AlCl3 6H2O in 2 L water. A large amount of white precipitate was observed. The precipitate was filtered and dried to a constant weight in an oven at 105° C. A white powder, aluminum salt of diisobutylphosphinic acid, of 139.43 g was obtained. The yield was 98.9%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08097747B2 |
| 出典データセット | uspto-grants-2012_01 |
| ORD ID | ord-d2d3394aca7145b0bec458126a88fb35 |
| 出典メモ | uspto-grants-2012_01 |