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Sulfuric Acid → 4-Amino-3-nitrobenzophenone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | 4-Acetamido-3-nitrobenzophenone | HCID 596969 | — |
| 生成物 | 4-Amino-3-nitrobenzophenone | HCID 596970 | — |
反応手順
Ten grams of 4-acetamido-3-nitrobenzophenone were added portionwise to 40 ml. of sulfuric acid. The reaction temperature was moderated with a water bath. After stirring about 45 minutes the reaction mixture was carefully poured over ice. The precipitated product was filtered to yield 4-amino-3-nitrobenzophenone.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04401817 |
| 出典データセット | uspto-grants-1983_08 |
| ORD ID | ord-4f2cc8e00d8145e98418d2bf2ce66346 |
| 出典メモ | uspto-grants-1983_08 |