化工社化工社 化学情報印刷レポート · 研究参考用
Potassium Hydroxide → N,N'-Heptamethylenebis(4-isopropoxybenzamide)
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | 1,7-Heptanediamine | HCID 69533 | — |
| 反応物 | 4-Isopropoxybenzoyl chloride | HCID 2724465 | — |
| 溶媒 | 1,2-Dichloroethane | HCID 11 | — |
| 生成物 | N,N'-Heptamethylenebis(4-isopropoxybenzamide) | HCID 21452919 | — |
反応手順
m.p. 135°-136° C., 10.9 g., was prepared as in Example 1 using a solution of 4-isopropoxybenzoyl chloride (from 18.0 g. of 4-isopropoxybenzoic acid as in Example 6) in 100 ml. of ethylene dichloride, 8.9 g. of 1,7-heptanediamine, 200 ml. of 10% aqueous potassium hydroxide solution, 500 ml. ethylene dichloride and recrystallization from acetonitrile using decolorizing charcoal.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04009208 |
| 出典データセット | uspto-grants-1977_02 |
| ORD ID | ord-91a8fc79e8c046b988e192deb662d36c |
| 出典メモ | uspto-grants-1977_02 |