関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 1,3-Butadiene | HCID 7845 | — |
| 反応物 | Phenylmaleic anhydride | HCID 99174 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | 1-Phenyl-4-cyclohexene-1,2-dicarboxylic acid anhydride | HCID 12679904 | — |
反応手順
A mixture of α-phenyl-maleic anhydride (20 g, 0.115 moles), butadiene (40 g, 0.74 moles) and 200 ml of toluene was heated at 100° C. in a sealed bomb for 15 hrs. The toluene solution was decanted from an insoluble, polymeric material and evaporated in vacuo to yield crude 1-phenyl-4-cyclohexene-1,2-dicarboxylic acid anhydride, bp 155° (0.3 mm).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04042707 |
|---|
| 出典データセット | uspto-grants-1977_08 |
|---|
| ORD ID | ord-c37bfb081e7f41c9b948d30a2b36e182 |
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| 出典メモ | uspto-grants-1977_08 |
|---|
