化工社化工社 化学情報印刷レポート · 研究参考用
Ethanol → ethyl 2-(4-cyanobenzoyl)-2-(9H-thioxanthen-9-yl)acetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | 9H-thioxanthen-9-ol | HCID 5154170 | — |
| 反応物 | Ethyl 2-(4-cyanobenzoyl)-2-(9H-thioxanthen-9-yl)acetate Ethyl-4-cyanobenzoyl acetate | HCID 131721214 | — |
| 溶媒 | Acetic Acid | HCID 176 | — |
| 生成物 | ethyl 2-(4-cyanobenzoyl)-2-(9H-thioxanthen-9-yl)acetate | HCID 54398664 | — |
反応手順
Ethyl 2-(4-cyanobenzoyl)-2-(9H-thioxanthen-9-yl)acetate Ethyl-4-cyanobenzoyl acetate (6 g, 28 mmol) and 9-hydroxy thioxanthene (6.6 g, 31 mmol) were mixed in acetic acid (50 ml) and ethanol (50 ml) using the procedure described in Example 3 (ii) to give ethyl 2-(4-cyanobenzoyl)-2-(9H-thioxanthen-9-yl)acetate as a pale yellow solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05891899 |
| 出典データセット | uspto-grants-1999_04 |
| ORD ID | ord-200afce35b8c4cbdbd597f47e8853533 |
| 出典メモ | uspto-grants-1999_04 |