化工社化工社 化学情報印刷レポート · 研究参考用
Nitrourea → Diethyl 2-(3-hydroxy-3-(p-biphenylyl)-propylamino)nonanedioate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Nitrourea | HCID 62372 | — |
| 反応物 | 1,4-Pentadien-3-one | HCID 543199 | — |
| 反応物 | Diethyl 2-(3-oxo-3-(p-biphenylyl)propylamino)nonanedioate | HCID 70578184 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | Diethyl 2-(3-hydroxy-3-(p-biphenylyl)-propylamino)nonanedioate | HCID 70510532 | — |
反応手順
A solution of diethyl 2-(3-hydroxy-3-(p-biphenylyl)-propylamino)nonanedioate (5 g), which was prepared via diethyl 2-(3-oxo-3-(p-biphenylyl)propylamino)nonanedioate from the appropriate vinyl ketone using the procedure of Example 2, in absolute ethanol (20 ml) was heated at 60° while nitrourea (1.12 g) was added portion-by-portion.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04262128 |
| 出典データセット | uspto-grants-1981_04 |
| ORD ID | ord-7d53ce85b93c416e9ea091733dd1cfec |
| 出典メモ | uspto-grants-1981_04 |