化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → 3-[(1-Methylpiperidin-4-yl)oxy]aniline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | N-[3-(1-Methyl-piperidin-4-yloxy)-phenyl]-acetamide | HCID 57444159 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 3-[(1-Methylpiperidin-4-yl)oxy]aniline | HCID 39202654 | — |
反応手順
A solution of N-[3-(1-Methyl-piperidin-4-yloxy)-phenyl]-acetamide (2.604 g) in absolute ethanol (40 mL) was treated with 37% hydrochloric acid and the solution was heated to reflux for 3 hours.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08541429B2 |
| 出典データセット | uspto-grants-2013_09 |
| ORD ID | ord-6031bf9140c847b7b1fab5f57e68279e |
| 出典メモ | uspto-grants-2013_09 |