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2-Bromo-1-methyl-1H-imidazole → 4-Methoxy-2-(1-methylimidazol-2-yl)benzo(b)furan
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Bromo-1-methyl-1H-imidazole | HCID 2773262 | — |
| 反応物 | 4-Methoxy-2-(trimethylstannyl)benzo(b)furan | HCID 22729126 | — |
| 生成物 | 4-Methoxy-2-(1-methylimidazol-2-yl)benzo(b)furan | HCID 22729146 | 53.4% |
反応手順
By the reactions in the same manner as in Starting Material Synthesis Example 87 using 4-methoxy-2-(trimethylstannyl)benzo(b)furan (5.26 g), 2-bromo-1-methylimidazole (2.72 g) and bistriphenylphosphinepalladium dichloride (593 mg), the title compound (2.06 g) was obtained as a yellow oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07196199B2 |
| 出典データセット | uspto-grants-2007_03 |
| ORD ID | ord-c0ae3ad54bfe48909422715b0dadf4a9 |
| 出典メモ | uspto-grants-2007_03 |