化工社化工社 化学情報印刷レポート · 研究参考用
1-Octene → Gamma-Decalactone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Octene | HCID 8125 | — |
| 反応物 | Potassium Acetate | HCID 517044 | — |
| 溶媒 | Acetic Acid | HCID 176 | — |
| 生成物 | Gamma-Decalactone | HCID 12813 | 48% |
反応手順
Octene-1 in an amount of 2.2 g. and 23.6 g. of ceric ammonium nitrate, Ce(NH4)2 (NO3)6, were refluxed under nitrogen in 200 ml. glacial acetic acid containing 60 g. potassium acetate for less than 0.5 hour, there being obtained a 48% yield of gamma-n-hexyl-butyrolactone.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04175089 |
| 出典データセット | uspto-grants-1979_11 |
| ORD ID | ord-2c03d4a37bfe48c9975a949c07039ab8 |
| 出典メモ | uspto-grants-1979_11 |