関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Benzaldehyde | HCID 240 | — |
| 反応物 | Isobutyric anhydride | HCID 7346 | — |
| 反応物 | Sodium Cyanide | HCID 8929 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Cyano(phenyl)methyl 2-methylpropanoate | HCID 13536647 | — |
反応手順
A 100-ml round-bottomed flask equipped with a magnetic stirrer was charged with isobutyric anhydride (10 mmol), benzaldehyde (10 mmol), a mixture of alkanes (25 ml) having a boiling range of from 62° C. to 82° C., sodium cyanide (12 mmol) and water (3 ml). The mixture formed was stirred at a temperature of 25° C. The table presents the yields of the title ester after the reaction times indicated (Embodiment IV).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US04175094 |
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| 出典データセット | uspto-grants-1979_11 |
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| ORD ID | ord-b8b0d7af08bb45c5b88e08b5a8efd0a7 |
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| 出典メモ | uspto-grants-1979_11 |
|---|