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HRID 46753作成日:2026年10月24日

Benzaldehyde → Cyano(phenyl)methyl 2-methylpropanoate

https://huagongshe.com/ja/reaction/46753

反応式

関与物質

役割名称HCID仕込み量
反応物BenzaldehydeHCID 240—
反応物Isobutyric anhydrideHCID 7346—
反応物Sodium CyanideHCID 8929—
溶媒WaterHCID 962—
生成物Cyano(phenyl)methyl 2-methylpropanoateHCID 13536647—

反応条件

温度25 °C

反応手順

A 100-ml round-bottomed flask equipped with a magnetic stirrer was charged with isobutyric anhydride (10 mmol), benzaldehyde (10 mmol), a mixture of alkanes (25 ml) having a boiling range of from 62° C. to 82° C., sodium cyanide (12 mmol) and water (3 ml). The mixture formed was stirred at a temperature of 25° C. The table presents the yields of the title ester after the reaction times indicated (Embodiment IV).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04175094
出典データセットuspto-grants-1979_11
ORD IDord-b8b0d7af08bb45c5b88e08b5a8efd0a7
出典メモuspto-grants-1979_11