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Potassium Carbonate → HCID 178472280、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | HCID 178418336 | HCID 178418336 | — |
| 反応物 | HCID 178472284 | HCID 178472284 | — |
| 溶媒 | Water | HCID 962 | — |
| 溶媒 | Diethyl Ether | HCID 3283 | — |
| 生成物 | HCID 178472280 | HCID 178472280 | — |
反応手順
By a procedure analogous to that of Example 1, but using 1.96 g of ethyl diethoxymethylphosphinate and 20 ml of a molar solution of benzylmagnesium chloride in diethyl ether and adding 4.14 g of potassium carbonate in 5 ml of water to precipitate inorganic salts, benzyl (diethoxymethyl) phosphine oxide is obtained as a colourless oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05298663 |
| 出典データセット | uspto-grants-1994_03 |
| ORD ID | ord-fd52caa51c214f8ea9275e21ac0c4034 |
| 出典メモ | uspto-grants-1994_03 |