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N,N'-di-sec-butylidene-4,4'-methylenebis(2,6-diethylbenzeneamine) → N,N'-di-sec-butyl-4,4'-methylenebis(2,6-diethylbenzeneamine)
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N,N'-di-sec-butylidene-4,4'-methylenebis(2,6-diethylbenzeneamine) | HCID 86608152 | — |
| 触媒 | Platinum | HCID 23939 | — |
| 溶媒 | Acetone | HCID 180 | — |
| 生成物 | N,N'-di-sec-butyl-4,4'-methylenebis(2,6-diethylbenzeneamine) | HCID 66781129 | — |
反応手順
N,N′-di-sec-butylidene-4,4′-methylenebis(2,6-diethylbenzeneamine) (22.53 g) and Pt(S)/C (2.65 g) were added to acetone (34.0 g) in an autoclave. The closed autoclave was purged 3 times with 125 psig of H2 (9.63×105 Pa) at 22° C. The mixture was kept at 21° C. and 125 psi (8.62×105 Pa) of H2 for 6.5 hours, forming the corresponding N,N′-di-sec-butyl-4,4′-methylenebis(2,6-diethylbenzeneamine) quantitatively.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07767858B2 |
| 出典データセット | uspto-grants-2010_08 |
| ORD ID | ord-89a1f47fe05b44cb85f0618e9dc4766f |
| 出典メモ | uspto-grants-2010_08 |