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HRID 52052作成日:2026年10月24日

Acetic Anhydride → N-[4-(4-Piperidinomethyl-2-pyridyloxy)-cis-2-butenyl]-4-(2-acetoxyethylthio)butyramide

https://huagongshe.com/ja/reaction/52052

反応式

関与物質

役割名称HCID仕込み量
反応物Acetic AnhydrideHCID 7918—
反応物N-[4-(4-Piperidinomethyl-2-pyridyloxy)-cis-2-butenyl]-4-(2-hydroxyethylthio)butyramideHCID 67725591—
生成物N-[4-(4-Piperidinomethyl-2-pyridyloxy)-cis-2-butenyl]-4-(2-acetoxyethylthio)butyramideHCID 6772558680%

反応手順

Following a procedure similar to that described in Example 2, but using N-[4-(4-piperidinomethyl-2-pyridyloxy) -cis-2-butenyl]-4-(2-hydroxyethylthio)butyramide (prepared as described in Example 3) and acetic anhydride as starting materials, in relative proportions similar to those used in that Example, the title compound, melting at 36°-40° C., was obtained in an 80% yield.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05616579
出典データセットuspto-grants-1997_04
ORD IDord-d9b235dc18d24b6588d5925c474fd755
出典メモuspto-grants-1997_04