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Ethyl formate → Formamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl formate | HCID 8025 | — |
| 反応物 | Methyl 3-carbamoylisobutyrate | HCID 11768702 | — |
| 生成物 | Formamide | HCID 713 | — |
| 生成物 | Methylsuccinic acid ethyl methyl ester | HCID 54001611 | — |
反応手順
The procedure in Example 3 (3) was repeated except that ethyl formate was used in place of methyl formate. As a result, the conversion of methyl 3-carbamoylisobutyrate was 83.7% and there were obtained methylsuccinic acid ethyl methyl ester at a selectivity of 99.8% and formamide at a selectivity of 98.6%, each based on the reacted methyl 3-carbamoylisobutyrate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05618953 |
| 出典データセット | uspto-grants-1997_04 |
| ORD ID | ord-0b2414389f2d435ebd782a575159d2a6 |
| 出典メモ | uspto-grants-1997_04 |