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4-Chloro-2-phenyl-pyrimidine-5-carboxylic acid (2-diethylamino-ethyl)-amide → HCID 178418472、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Chloro-2-phenyl-pyrimidine-5-carboxylic acid (2-diethylamino-ethyl)-amide | HCID 53745902 | — |
| 反応物 | Sodium hydrogen sulphide | HCID 86586439 | — |
| 生成物 | HCID 178418472 | HCID 178418472 | 63.6% |
反応手順
Using the procedure in Preparation 34, 6.4 g (0.02 mol) of 4-chloro-2-phenyl-pyrimidine-5-carboxylic acid (2-diethylamino-ethyl)-amide was reacted with 4.8 g (0.066 mol) of sodium hydrogen sulfide to afford 4.2 g of the title compound, mp 178°-180° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05620997 |
| 出典データセット | uspto-grants-1997_04 |
| ORD ID | ord-10fcd818c14448c6a46b2fe2efcb38fe |
| 出典メモ | uspto-grants-1997_04 |