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1-Fluoro-2-iodo-4-nitrobenzene → Benzyl 4-[(2-iodo-4-nitrophenyl)amino]piperidine-1-carboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Fluoro-2-iodo-4-nitrobenzene | HCID 10539733 | — |
| 反応物 | 4-Amino-1-N-Cbz-piperidine | HCID 17846640 | — |
| 生成物 | Benzyl 4-[(2-iodo-4-nitrophenyl)amino]piperidine-1-carboxylate | HCID 57962346 | 64% |
反応手順
The desired compound was prepared according to the procedure of Example D83, step A, using 1-fluoro-2-iodo-4-nitrobenzene and benzyl 4-aminopiperidine-1-carboxylate as the starting materials in 64% yield. LCMS for C19H211N3O4 (M+H)+: m/z=482.0.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08871753B2 |
| 出典データセット | uspto-grants-2014_10 |
| ORD ID | ord-56df9b28f56941dbae0db95e2f1cdde6 |
| 出典メモ | uspto-grants-2014_10 |