化工社化工社 化学情報印刷レポート · 研究参考用
Homoveratrylamine → N-[2-(3,4-dimethoxyphenyl)ethyl]-2-(N,N-diphenylamino)acetamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Homoveratrylamine | HCID 8421 | — |
| 反応物 | (Diphenylamino)acetic acid | HCID 735138 | — |
| 溶媒 | Ethyl Acetate | HCID 8857 | — |
| 生成物 | N-[2-(3,4-dimethoxyphenyl)ethyl]-2-(N,N-diphenylamino)acetamide | HCID 20460535 | 66.9% |
反応手順
3,4-Dimethoxyphenethylamine (8.05 g) and N,N-diphenylglycine (10 g) were heated for 2 hours at 190° C. After cooling, the reaction mixture was dissolved in ethylacetate. The resulting solution was washed with a 5% sodium bicarbonate aqueous solution and water and then dried. The solvent was distilled off from the solution to give crystals of N-[2-(3,4-dimethoxyphenyl)ethyl]-2-(N,N-diphenylamino)acetamide (11.5 g), mp 88° to 93° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04447436 |
| 出典データセット | uspto-grants-1984_05 |
| ORD ID | ord-45297bd446e64c57a8b8e214217fb816 |
| 出典メモ | uspto-grants-1984_05 |