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Pyridine → HCID 178444542、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Pyridine | HCID 1049 | — |
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | HCID 178444557 | HCID 178444557 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | HCID 178444542 | HCID 178444542 | — |
反応手順
20 mL of thionyl chloride was added dropwise to a mixture containing 20.0 g (0.1 mol) of trans-4-pentylcyclohexanecarboxylic acid represented by the following formula (b-i), 0.5 mL of pyridine and 300 mL of toluene in a nitrogen atmosphere, and the mixture was stirred under heating to 80° C. or less for 1 hour. The solvent was distilled off under reduced pressure to provide trans-4-pentylcyclohexanecarboxylic acid chloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08048335B2 |
| 出典データセット | uspto-grants-2011_11 |
| ORD ID | ord-ca2f9cd410f44863bb2746a888088958 |
| 出典メモ | uspto-grants-2011_11 |