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Ethyl 3-formyl-4-methoxybenzoate → 4-methoxy-3-[(E)-2-(4-trifluoromethylphenyl)vinyl]benzoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl 3-formyl-4-methoxybenzoate | HCID 638670 | — |
| 反応物 | Diethyl 4-(trifluoromethyl)benzylphosphonate | HCID 15819199 | — |
| 反応物 | ethyl 4-methoxy-3-[(E)-2-(4-trifluoromethylphenyl)vinyl]-benzoate | HCID 23141481 | — |
| 生成物 | 4-methoxy-3-[(E)-2-(4-trifluoromethylphenyl)vinyl]benzoic acid | HCID 23141489 | — |
反応手順
The captioned compound was synthesized from ethyl 4-methoxy-3-[(E)-2-(4-trifluoromethylphenyl)vinyl]-benzoate, which had been synthesized from diethyl (4-trifluoromethylbenzyl)phosphonate and ethyl 3-formyl-4-methoxybenzoate obtained in step C of Example 1-2-1, in accordance with the same procedure as in the methods described in step B of Example 2-2-1.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08063046B2 |
| 出典データセット | uspto-grants-2011_11 |
| ORD ID | ord-9af344e05e8140a5a4c65a517c7f0d86 |
| 出典メモ | uspto-grants-2011_11 |