関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Imidazole | HCID 795 | — |
| 反応物 | Ethylene carbonate | HCID 7303 | — |
| 反応物 | 2,6-Dichloro-4-methylphenol | HCID 17077 | — |
| 生成物 | 2-(2,6-Dichloro-4-methylphenoxy)ethan-1-ol | HCID 21396902 | — |
反応手順
2,6-Dichloro-4-methylphenol (1 eq.), ethylene carbonate (1 eq.) and imidazole (0.5% loading) were combined and heated at 150° C. for 4 h to afford the title compound as a brown oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US08063105B2 |
|---|
| 出典データセット | uspto-grants-2011_11 |
|---|
| ORD ID | ord-1ab1a93deda14501b292e7f6ce123d80 |
|---|
| 出典メモ | uspto-grants-2011_11 |
|---|
