関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Calcium Carbonate | HCID 10112 | — |
| 反応物 | 3-(1-Bromoethyl)benzophenone | HCID 12802924 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 3-(1-Hydroxyethyl)benzophenone | HCID 13102751 | — |
反応手順
In an autoclave, 100 ml of water and 3.3 g of calcium carbonate and 10 g of 3-(1-bromoethyl)benzophenone were placed, and were then heated at 120° C. for 6 hours. The resultant reaction solution was extracted with benzene, and a formed benzene layer was then dried with anhydrous sodium sulfate, followed by distilling off the solvent. The resultant product had the spectrum data which were identical with those of 3-(1-hydroxyethyl)benzophenone.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04734528 |
|---|
| 出典データセット | uspto-grants-1988_03 |
|---|
| ORD ID | ord-fa741a064cc14d138e326f1101822562 |
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| 出典メモ | uspto-grants-1988_03 |
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