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Potassium Carbonate → Methyl 4-amino-3-(4-chlorocinnamylamino)benzoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | 3,5-Diamino-2-methylbenzoic acid | HCID 135524 | — |
| 反応物 | p-Chlorocinnamyl chloride | HCID 53728250 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | Methyl 4-amino-3-(4-chlorocinnamylamino)benzoate | HCID 53813638 | 63.2% |
反応手順
5.0 g of methyl 3,4-diaminobenzoate was dissolved in 40 ml of dimethylformamide, and to the solution were added 2.07 g of potassium carbonate and 1.87 g of p-chlorocinnamyl chloride, and reaction was carried out according to the procedure in Reference Example 40, to obtain 2.0 g of the title compound as a light brown oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05245034 |
| 出典データセット | uspto-grants-1993_09 |
| ORD ID | ord-02666c15032d4a23816abf9f01b6ac87 |
| 出典メモ | uspto-grants-1993_09 |