化工社化工社 化学情報印刷レポート · 研究参考用
1-Vinyl-2-trifluoromethyl-2,3,3-trifluorocyclobutane → Benzene, 1-fluoro-2-(trifluoromethyl)-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Vinyl-2-trifluoromethyl-2,3,3-trifluorocyclobutane | HCID 20134582 | — |
| 溶媒 | Benzene | HCID 241 | — |
| 生成物 | Benzene, 1-fluoro-2-(trifluoromethyl)- | HCID 9807 | 41% |
反応手順
The general procedure was followed using 11.0 g of 1-vinyl-2-trifluoromethyl-2,3,3-trifluorocyclobutane dissolved in 11.15 g of benzene as the liquid feed at a flow rate of 1 ml/hr. Nitrogen was used as the inert carrier. The reactor was charged with 2.0 g of activated carbon. At 400° C. 41% of o-trifluoromethylfluorobenzene was produced.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04754084 |
| 出典データセット | uspto-grants-1988_06 |
| ORD ID | ord-39825371865942a4b6ee94c2fdc6ef8a |
| 出典メモ | uspto-grants-1988_06 |