関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | N-(4-bromo-2-nitrophenyl)acetamide | HCID 136690 | — |
| 溶媒 | 1,2-Dimethoxyethane | HCID 8071 | — |
| 生成物 | 4-Bromo-2-nitroaniline | HCID 70132 | — |
反応手順
A mixture of 1d (3.5 g, 13.5 mmol), dimethoxyethane (100 ml) and aqueous sodium hydroxide (50 ml, 1 M) is heated to 80° C. for 1 hour. After cooling the mixture is poured into ice-water. The product is filtered off, washed with water and dried. Yield 2.77 g (94%). Mp 109-1 10° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05922724 |
|---|
| 出典データセット | uspto-grants-1999_07 |
|---|
| ORD ID | ord-ce5c175808de4d54af57312909f4641a |
|---|
| 出典メモ | uspto-grants-1999_07 |
|---|
