化工社化工社 化学情報印刷レポート · 研究参考用
Oxalyl chloride → 2-Chloro-6-methylbenzoyl isocyanate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Oxalyl chloride | HCID 65578 | — |
| 反応物 | Benzamide, 2-chloro-6-methyl- | HCID 113589 | — |
| 溶媒 | 1,2-Dichloroethane | HCID 11 | — |
| 生成物 | 2-Chloro-6-methylbenzoyl isocyanate | HCID 90019597 | 86.7% |
反応手順
The title compound was prepared according to the procedure described in step-2 of Intermediate-8 by using 2-chloro-6-methylbenzamide (1.0 g, 5.9 mmol), oxalyl chloride (0.894 g, 7.1 mmol) and EDC (20 mL) to afford 1.00 g of the desired product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09439890B2 |
| 出典データセット | uspto-grants-2016_09 |
| ORD ID | ord-1eea1c649c4e4c389264d24d65d8cc40 |
| 出典メモ | uspto-grants-2016_09 |