関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Lithium Hydroxide | HCID 3939 | — |
| 反応物 | Methyl Stearate | HCID 8201 | — |
| 反応物 | (1-2-Hydroxyethyl)-2,2,6,6-tetramethyl-4-hydroxymethyl-piperidine | HCID 53937473 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 1-(2-Stearoyloxyethyl)-2,2,6,6-tetramethyl-4-methyl piperidine stearate | HCID 21292218 | — |
反応手順
9.8 g of 1-(2-hydroxyethyl)-2,2,6,6-tetramethyl-4-hydroxymethyl piperidine as obtained in Example 2 (0.045 mole) were admixed to 28.7 g of methyl stearate (0.09 mole) in the presence of 0.5 g of LiOH. The mixture was heated to 140° C. in a nitrogen atmosphere and was maintained under stirring until complete evolvement of the reaction methyl alcohol.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04772708 |
|---|
| 出典データセット | uspto-grants-1988_09 |
|---|
| ORD ID | ord-25f8bacf134a4b57be107a0a1eefb2ff |
|---|
| 出典メモ | uspto-grants-1988_09 |
|---|
