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3-Hydrazinopyridine → HCID 178479606、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Hydrazinopyridine | HCID 10909519 | — |
| 反応物 | Ethyl 4-chloro-1,6-naphthyridine-3-carboxylate | HCID 17608818 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | HCID 178479606 | HCID 178479606 | — |
反応手順
A solution of 2.84 g of ethyl 4-chloro-1,6-naphthyridine-3-carboxylate and 1.35 g of 3-hydrazinopyridine in 36 ml of methanol is stirred at room temperature for 2.5 hours, then refluxed for 4.5 hours, then cooled in an ice bath and filtered. Collected solid is washed with methanol, then with ether to yield 2-(3-pyridyl)pyrazolo[4,3-c][1,6]naphthyridin-3-(5H)-one hydrochloride, m.p. 302°-305°.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04560689 |
| 出典データセット | uspto-grants-1985_12 |
| ORD ID | ord-563f916753134b21b4bc2f43d4041847 |
| 出典メモ | uspto-grants-1985_12 |