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Acetic Acid → Prenyl acetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetic Acid | HCID 176 | — |
| 反応物 | Phosphoric Acid | HCID 1004 | — |
| 反応物 | Isoprene | HCID 6557 | — |
| 生成物 | Prenyl acetate | HCID 14489 | — |
反応手順
Although the addition of acetic acid to isoprene in the presence of a catalytic amount of phosphoric acid will occur slowly at room temperature to yield prenyl acetate (systematically named as 3-methyl-2-buten-1-yl acetate), gentle heating of the reaction mixture in a pressure vessel at temperatures of approximately 40° C. to 100° C. is preferred if one wishes to conduct the process in several hours.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06278016B1 |
| 出典データセット | uspto-grants-2001_08 |
| ORD ID | ord-20493111b84f418998a68a4f717837f2 |
| 出典メモ | uspto-grants-2001_08 |